Separation of organotellurium compounds by method of reversed-phase thin-layer chromatography with FT-IR spectrometry detection

Authors

  • Elena V. Eliseeva postgraduate student, Department of organic, bioorganic and medical chemistry, Samara State University, Samara, email: eliseeff@mail.ru
  • Alexander A. Sorokin cand. chem. sci., deputy chief of the scientific research center for the development of analytical methods, Limited (liability) company «Ozon», Samara region, Zhigulevsk, e-mail: alanso@list.ru
  • Nikolay A. Red’kin cand. chem. sci., chief lecturer, Department of analytical and expert chemistry, Samara State University, Samara, email: xiredn@mail.ru
  • Vitaly P. Gar’kin cand. chem. sci., docent, Department of organic, bioorganic and medical chemistry, Samara State University, Samara, email: garkin@ssu.samara.ru

Keywords:

σ-and π-telluranes, reversed-phase thin-layer chromatography, infrared spectrometry with Fourier-transform.

Abstract

The influence of components of mobile phase on the sorption properties of σ-and π-telluranes in
conditions of reversed-phase thin-layer chromatography was investigated in study. Separation of model
mixture of compounds was carried out using two-dimensional RF TLC. It is shown that the use of FT-IR
spectrometry for the detection of compounds after TLC separation, allows us to identify the compounds and
to establish changes taking place with them during the elution.

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Published

2019-11-19

Issue

Vol. 14 No. 4 (2014): Sorbtsionnye i Khromatograficheskie Protsessy

Section

Статьи

How to Cite

Separation of organotellurium compounds by method of reversed-phase thin-layer chromatography with FT-IR spectrometry detection. (2019). Sorbtsionnye I Khromatograficheskie Protsessy, 14(4). https://journals.vsu.ru/sorpchrom/article/view/1522

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