Synthetical calcium hydroxyapatite and its natural analogues

Authors

  • Nikolay A. Zakharov head of the biocompatible materials sector; Doctor of Physical and Mathematical Sciences; senior research scientist; IGIC RAS; Moscow; e-mail: zakharov@igic.ras.ru
  • Maxim Ju. Sentsov PhD student; IGIC RAS; Moscow; e-mail: sentsov.maxim@gmail.com
  • Ljudmila I. Demina Cand. Sc. (Chemistry); senior research scientist; IGIC RAS; Moscow
  • Tat’yana V. Zakharova Cand. Sc. (Physics and Mathematics); associate professor; IGIC RAS; Moscow
  • Vladimir T. Kalinnikov head of the phosphate chemistry laboratory; academician; professor; IGIC RAS; Moscow

Keywords:

hydroxyapatite; phosphate; X-ray diffraction analysis; oscillation spectroscopy; crystalline structure.

Abstract

Stoichiometric calcium hydroxyapatite was synthesized from aqueuos solutions of calcium and
phosphorus salts. Composition and structure of the HAp and its natural analogues were determined by
XRD analysis, FTIR spectroscopy, electron microscopy and thermogravimetric analysis. As was shown,
natural apatites are characterized not only by presence of carbonate groups in their structure, but by
comprisal of diphosphate groups, oxygen and fluorine. It was determined that there is trace impurity of
iron, strontium, sodium and potassium in the natural apatites. In the current paper results of determination
of the structural, spectroscopic and thermal characteristics of the HAp and its natural analogues are
shown

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Published

2019-11-28

How to Cite

Synthetical calcium hydroxyapatite and its natural analogues. (2019). Sorbtsionnye I Khromatograficheskie Protsessy, 10(6). https://journals.vsu.ru/sorpchrom/article/view/2123

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