Process control synthesis of imidazolines of saturated fatty acids by TLC and GC/MS methods

Authors

  • А. А. Кружилин Kruzhilin Alexey A. – student, Department of Organic Chemistry, Voronezh State University, Voronezh
  • А. С. Перегудова Peregudova Alexandra S. — Postgraduate student, Department of Organic Chemistry, Voronezh State University, Voronezh
  • И. Э. Перелыгина Perelygina Inna E. – Postgraduate student, Department of Organic Chemistry, Voronezh State University, Voronezh
  • Н. В. Столповская Stolpovskaya Nadezhda V. – Associate professor, Department of Organic Chemistry, Voronezh State University, Voronezh
  • А. В. Фалалеев Falaleev Alexander V. - Ph. D., Senior Researcher, Voronezh State University, Voronezh

DOI:

https://doi.org/10.17308/sorpchrom.2015.15/295

Keywords:

thin layer chromatography, gas chromatography-mass spectrometry, imidazolines, saturated fatty acids

Abstract

The chromatographic procedures for control of imidazolines synthesis based on interaction of
saturated fatty acids on an example of caprylic, capric and myristic with aminoethylethanolamine have been
represented. The optimal conditions of the thin layer chromatography for the determination of the conversion
of fatty acids are proposed. The structure of obtained imidazolines has been determined by gas
chromatography-mass spectrometry.

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Published

2018-02-19

Issue

Vol. 15 No. 3 (2015): Sorption and chromatographic processes

Section

Статьи

How to Cite

Process control synthesis of imidazolines of saturated fatty acids by TLC and GC/MS methods. (2018). Sorbtsionnye I Khromatograficheskie Protsessy, 15(3), 464-472. https://doi.org/10.17308/sorpchrom.2015.15/295

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