SALDI Mass - spectrometry for research clusters as a part of poorly conducting deposits

Authors

  • Irina S. Goncharova postgraduate student, Institute of Physical Chemistry and Electrochemistry A.N. Frumkin, Russian Academy of Science, Moscow, e-mail: gis8801@yandex.ru
  • Aleksey K. Buryak Doctor of Chemical Sciences, professor, head of the Laboratory of Physical-chemical principles of chromatography and gas chromatography-mass spectrometry, Institute of Physical Chemistry and Electrochemistry A.N. Frumkin, Russian Academy of Science, Moscow
  • Ivan S. Pickii Candidate of Chemical Sciences, senior scientist, Institute of Physical Chemistry and Electrochemistry A.N. Frumkin, Russian Academy of Science, Moscow
  • Nikolay G. Ivanov Deputy department chief JSC «NPO Energomash named after academician V. Glushko», Khimky, Moscow region
  • Vladimir V. Fedorov Chief specialist of LPRE units department JSC «NPO Energomash named after academician V. Glushko», Khimky, Moscow region

Keywords:

clusters, MALDI/SALDI mass-spectrometry, poorly conducting deposits, surface chemistry.

Abstract

The method of Surface Assisted Laser Desorption/Ionization mass spectrometry is used to study
chemistry of poorly conducting deposits forming channels’ walls of the combustion chamber cooling path of
the liquid fuel rocket motor. Such deposits interfere with the operations temperature conditions of the
product, making difficult heat exchange. This method simplifies sample preparation and allows to obtain
deposits qualitative composition and the nature of metal clusters formed under "soft ionization" dates.

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Published

2019-11-21

How to Cite

SALDI Mass - spectrometry for research clusters as a part of poorly conducting deposits. (2019). Sorbtsionnye I Khromatograficheskie Protsessy, 13(5). https://journals.vsu.ru/sorpchrom/article/view/1674

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