Diaryltellurimides investigation by HPLC-MS method and by direct inlet in mass-spectrometric detector

Authors

  • Tatyana A. Rodina senior scientist, Russian academy of sciences A.N. Frumkin Institute of Physical Chemistry and Electrochemistry, E-mail: rodina@front.ru
  • Vitaliy P. Gar`kin Vice Rector for Academic Affairs, State educational institution of higher education Samara State University, Samara, tell. (8462) 334-54-05, fax: (8462) 334-54-17
  • Aleksey K. Buryak head of laboratory, Russian academy of sciences A.N. Frumkin Institute of Physical Chemistry and Electrochemistry

Keywords:

diaryltellurimides, reserved phase high performance liquid chromatography with mass spectrometry detection, direct inlet in the mass spectrometric detector, electrospray ionization.

Abstract

The behavior of a number of diaryltellurimids in different variants of HPLC has been
investigated. It is found out that the compounds are hydrolyzed to the initial components in condition of
RP HPLC. It has been shown the possibility of investigation of the unstable compounds using direct inlet
in mass spectrometric detector. The mass spectra of investigated compounds at various applied voltage to
the “capillary” of mass spectrometric detector have been obtained and interpreted. The generalized
fragmentation scheme has been presented

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Published

2019-11-27

Issue

Vol. 10 No. 2 (2010): Sorbtsionnye i Khromatograficheskie Protsessy

Section

Статьи

How to Cite

Diaryltellurimides investigation by HPLC-MS method and by direct inlet in mass-spectrometric detector. (2019). Sorbtsionnye I Khromatograficheskie Protsessy, 10(2). https://journals.vsu.ru/sorpchrom/article/view/2036

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