Analysis of 1,1-dimethylhydrazine as its derivatives with isothiocyanates by off-line HPLC – MALDI-MS method

Authors

  • Sergei A. Paramonov post-graduate student, Institution of Russian Academy of Science A.N. Frumkin Institute Of Physical Chemistry And Electrochemistry of RAS, Moscow, e-mail: chrom-ms@mail.ru
  • Aleksey V. Uleanov Dr. Sc. Chem, Institution of Russian Academy of Science A.N. Frumkin Institute Of Physical Chemistry And Electrochemistry of RAS, Moscow
  • Aleksey K. Buryak Chief of laboratory, Dr. Sc. Chem., Institution of Russian Academy of Science A.N. Frumkin Institute Of Physical Chemistry And Electrochemistry of RAS, Moscow

Keywords:

high performance liquid chromatography, matrix-assisted laser/desorption/ionsation mass spectrometry, 1,1-dimethylhydrazine, thiosemicarbazides.

Abstract

The analysis possibility of 1,1-dimethylhydrazine as its derivatives with isothiocyanates was
reported. Influence of chromatographic system parameters on retention characteristics was investigated.
Using of matrix-assisted laser/desorption/ionsation mass spectrometry method in qualitative analysis of
1,1-dimethylhydrazine was studied.

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Published

2019-11-27

How to Cite

Analysis of 1,1-dimethylhydrazine as its derivatives with isothiocyanates by off-line HPLC – MALDI-MS method. (2019). Sorbtsionnye I Khromatograficheskie Protsessy, 10(3). https://journals.vsu.ru/sorpchrom/article/view/2065

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