Hydrothermal assisted conventional sol-gel method for synthesis of bioactive glass 70S30Cы

Keywords: Bioactive glass, Hydrothermal assisted sol-gel, Bioactivity, in vitro, Cell viability

Abstract

Bioactive glasses (Bioglasses) are widely synthesized by the conventional sol-gel method consisting of two main steps for sol and gel formation. However, the conversion from sol to gel requires a long time (5–7 days). In this study, the hydrothermal system was used to quickly synthesize the bioactive glass by reducing the conversion time from sol to gel. The hydrothermal assisted conventional sol-gel method was applied for synthesis of the bioactive glass 70SiO2–30CaO (mol%) (noted as 70S30C). The synthetic glass was investigated by the physical-chemical techniques. The ‘‘in vitro’’ experiments in SBF (Simulated Body Fluid) solution was also performed to evaluate the bioactivity of synthetic material. The obtained results show that the bioactive glass 70S30C was successfully elaborated by using the hydrothermal assisted conventional sol-gel
method. The consuming time was reduced compared to the conventional method. The physical-chemical characterization confirmed that the synthetic glass is amorphous material with mesoporous structure consisting of interconnected particles.
The specific surface area, pore volume and average pore diameter of synthetic glass were 142.8 m2/g, 0.52 cm3/g, and 19.1 nm, respectively. Furthermore, synthetic bioactive glass exhibited interesting bioactivity when immersed in simulated body fluid (SBF) solution for 1 days and good biocompatibility when cultured in cellular media.

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Author Biographies

Ta Anh Tuan, Faculty of Chemical Technologies, Kazan National Research Technological University, 68 ul. K. Marksa, Kazan 420015, Tatarstan, Russian Federation

PhD student, Faculty of Chemical
Technologies, Kazan National Research Technological
University, Kazan, Tatarstan, Russian Federation;
email: taanhtuan84pt@hpu2.edu.vn

Elena V. Guseva, Faculty of Chemical Technologies, Kazan National Research Technological University, 68 ul. K. Marksa, Kazan 420015, Tatarstan, Russian Federation

PhD in Chemistry, Associate
Professor, Faculty of Chemical Technologies, Kazan
National Research Technological University, Kazan,
Tatarstan, Russian Federation; email: leylaha@mail.ru

Nguyen Anh Tien, Faculty of Chemistry, Ho Chi Minh City University of Education, 280 An Dương Vương str., Ward 4, District 5, Ho Chi Minh City, Vietnam

PhD in Chemistry, Associate
Professor, Chief of General and Inorganic Chemistry
Department, Ho Chi Minh City University of Education,
Vietnam; e-mail: tienna@hcmue.edu.vn

Ha Tuan Anh, Thu Dau Mot University, 6 Tran Van On str., Phu Hoa Ward, Thu Dau Mot City, Binh Duong Province 820000, Viet Nam

Thu Dau Mot University, Thu Dau
Mot City, Vietnam; e-mail: anhht@tdmu.edu.vn

Bui Xuan Vuong, Faculty of Pedagogy in Natural Sciences, Sai Gon University, Ho Chi Minh City, Vietnam

Associate Professor, Faculty of
Natural Sciences, Sai Gon University, Ho Chi Minh City,
Vietnam; e-mail: bxvuong@sgu.edu.vn

Le Hong Phuc, Institute of Applied Mechanics and Informatics, 291 Dien Bien Phu str., District 03, Ho Chi Minh City 700000, Vietnam

Institute of Applied Mechanics and
Informatics, Ho Chi Minh City, Vietnam; e-mail:
lhphuc@hcmip.vast.vn

Nguyen Quan Hien, Institute of Applied Mechanics and Informatics, 291 Dien Bien Phu str., District 03, Ho Chi Minh City 700000, Vietnam

Ho Chi Minh City Institute of
Physics, Vietnam Academy of Science and Technology,
Ho Chi Minh City, Vietnam; e-mail: quanhiengv@yahoo.com.vn

Bui Thi Hoa, Institute of Theoretical and Applied Research, Duy Tan University, Hanoi 100000, Vietnam; Faculty of Natural Sciences, Duy Tan University, Da Nang 550000, Vietnam

Institute of Theoretical and Applied
Research, Duy Tan University, Hanoi, Vietnam; Faculty
of Natural Sciences, Duy Tan University, Da Nang,
Vietnam; e-mail: buithihoa2@duytan.edu.vn

Nguyen Viet Long, Department of Electronics and Telecommunication, Sai Gon University, Ho Chi Minh City 700000, Vietnam

Department of Electronics and
Telecommunication, Sai Gon University, Ho Chi Minh
City, Vietnam; e-mail: nguyenviet_long@yahoo.com

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Published
2021-11-24
How to Cite
Tuan, T. A., Guseva, E. V., Tien, N. A., Anh, H. T., Vuong, B. X., Phuc, L. H., Hien, N. Q., Hoa, B. T., & Long, N. V. (2021). Hydrothermal assisted conventional sol-gel method for synthesis of bioactive glass 70S30Cы. Kondensirovannye Sredy I Mezhfaznye Granitsy = Condensed Matter and Interphases, 23(4), 585-593. https://doi.org/10.17308/kcmf.2021.23/3678
Section
Original articles