ФИЗИКО-ХИМИЧЕСКИЕ СВОЙСТВА СУЛЬФАТНО-ГЛИЦИНАТНЫХ РАСТВОРОВ ЦИНКОВАНИЯ
Ключевые слова:
электролит цинкования, глицин, электропроводность, оптическая плотность, энтальпия активации вязкого течения, комплексообразование, координационное число
Аннотация
Изучены физико-химические свойства сульфатно – глицинатных электролитов, проведена оценка взаимодействия компонентов в изучаемых растворах цинкования при содержании ZnSO4 0.05-0.25 моль/л, NH2CH2COOH 0.6-0.95 моль/л в диапазоне температур 22-55 °С. На основании анализа зависимости электропроводности, оптической плотности, вязкости и энтальпии вязкого течения от состава растворов обоснован выбор концентраций компонентов модельного электролита цинкования.
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Литература
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2. Shehanov R. F., Gridchin S. N., Balmasov A. V., Rumjanceva K. E. Russian Journal of Chemistry and Chemical Technology [Izv. vuzov. Himija i himicheskaja tehnologija], 2015, vol. 58, no. 1, pp. 104-106. (in Russian)
3. Bobrikova I. G., Goncharenko E. G., Shahlevich E. S. Modern Tends in the Development of Science and Technology, 2016, no. 3-3, pp. 28-31. (in Russian)
4. Shmidt V. V., Zhihareva I. G., Rakashov A. A. Scientific and Technical “Volga Region Bulletin”, 2015, no. 3, pp. 74-78. Available at: https://elibrary.ru/download/elibrary_23930413_17810952.pdf (accessed 21.09.2017). (in Russian)
5. Micin S., Martinez S., Malinovic B., Grozdanic V. Journal of Chemical Technology and Metallurgy, 2016, vol. 51, no. 5, pp. 556-562. Available at: http://dl.uctm.edu/journal/node/j2016-5/9-Micin_556-562.pdf (accessed 21.09.2017).
6. Berezin N. B., Berezina T. N., Mezhevich Zh. V., Sysoev V. A. Bulletin of the Technological University, 2014, vol. 17, no. 22, pp. 355 -359.
7. Petrushova O. Ju., Cupak T. E. Journal Adnvances in Chemistry and Chemical Technology, 2014, vol. XXVIII, no. 5, pp. 95-97. Available at: http://acct.muctr.ru/media/articles/pdf/2014_28_154_095-097.pdf (in Russian)
8. Dolgih O. V., Sockaja N. V., Shamanaeva E. S. Condensed Matter and Interphases, 2007, vol. 9, no. 1, pp. 32-39. Available at: http://www.kcmf.vsu.ru/resources/t_09_1_2007_006.pdf (in Russian)
9. Sapronova L. V., Sockaja N. V., Dolgih O. V. Condensed Matter and Interphases, 2013, vol. 15, no. 4, pp. 446-452. Available at: http://www.kcmf.vsu.ru/resources/t_15_4_2013_013.pdf (in Russian)
10. Berezin N. B., Berezina T. N., Mezhevich Zh. V., Chevela V. V. Bulletin of the Technological University, 2013, vol. 16, no. 5, pp. 267-268.
11. Kozihonov A. U., Dzhulaev U. N., Radzhabov U. R., Shukhratzoda M., Bobiev G. M. Reports of the Academy of Sciences of the Republic of Tajikistan, 2015, vol. 58, no. 7, pp. 608-614. Available at: https://elibrary.ru/download/elibrary_25600373_69170663.pdf (accessed 21.09.2017)
12. Berezin N. B., Gudin N. V., Filippova A. G., Chevela V. V., Mezhevich Zh. V., Jah'jaev Je. D., Sagdeev K. A. Electrodeposition of Metals and Alloys from Aqueous Solutions of Complex Compounds. Kazan, Kazan. State. Technol. University Publ., 2006, 276 p. (in Russian)
13. Mezhevich Zh. V., Berezin N. B. Bulletin of the Technological University, 2016, vol. 19, no. 9, pp. 51-53.
14. Krashhenko T. G., Vvedenshij A. V., Bobrinskaja E. V., Kuleshova N. E. Condensed Matter and Interphases, 2014, vol. 16, no. 1, pp. 42-49. Available at: http://www.kcmf.vsu.ru/resources/t_16_1_2014_007.pdf (in Russian)
15. Hohlov V. Ju, Selemenev V. F., Hohlova O. N, Zagorodnij A. A. Proceedings of Voronezh State University. Series: Chemistry. Biology. Pharmacy, 2003, no. 1, pp. 18-22. Available at: http://www.vestnik.vsu.ru/pdf/chembio/2003/01/hohlov.pdf (in Russian)
16. Bobreshkova O. V., Polumestnaya K. A., Fedosova A. A. Russian Journal of Electrochemistry, 2009, vol. 45, no. 3, pp. 345-349. DOI: 10.1134/S1023193509030161
17. Abrosimov V. K., Korolev V. V., Afanas'ev V. N., at al. Experimental Methods of Solution Chemistry: Densitometry, Viscosimetry, Conductometry and other Methods. Moscow, Science Publ.,1997, 351 p. (in Russian)
18. Solov`eva N. D., Frolova I. I., Legkaya D. A. Condensed Matter and Interphases, 2014, vol. 16, no. 2, pp. 201-205. Available at: http://www.kcmf.vsu.ru/resources/t_16_2_2014_013.pdf (in Russian)
19. Smirnov P. R., Trostin V. N. Structural Parameters of the Near Environment of Ions in Aqueous Solutions of Inorganic Electrolytes. Ivanovo, Ivanovo Publishing House, 2011, 400 p. (in Russian)
20. Kessler Ju. M., Petrenko V. E., Ljashhenko A. K., at al. / Ed. by Kutepov A. M. Water: Structure, Condition, Solvation. Achievements of Recent Years. Moscow, Science Publ., 2003, 404 p. (in Russian)
21. Bonaccorsi R., Palla P., Tomasi J. Journal of the American Chemical Society, 1984, vol. 106, no. 7, pp. 1945-1950. DOI: 10.1021/ja00319a008 Available at: http://pubs.acs.org/doi/abs/10.1021/ja00319a008 (accessed 21.09.2017)
22. Gorbitz C. H. Journal of the Chemical Society, Perkin Trans. 2, 1996, no. 10, pp. 2213-2219. DOI: 10.1039/P29960002213 Available at: http://pubs.rsc.org/-/content/articlepdf/1996/p2/p29960002213 (accessed 20.09.2017)
23. Kusalik P. G., Bergman D., Laaksonen A. Journal of Chemical Physics, 2000, vol. 113, no. 18, pp. 8036-8046. DOI: 10.1063/1.1315321 Available at: http://aip.scitation.org/doi/10.1063/1.1315321 (accessed 10.09.2017)
24. Kruchinin S. E. Thesis of Diss. ... Cand. Chem. Sci. Ivanovo, 2013, 155 pp. (in Russian)
25. Max J.-J., Chapados C. Journal of Physical Chemistry A, 2004, vol. 108, no. 16, pp. 3324-3337. DOI: 10.1021/jp036401t Available at: http://pubs.acs.org/doi/abs/10.1021/jp036401t (accessed 10.09.2017).
26. Afanas'ev V. N., Tjunina E. Ju., Rjabova V. V. Journal of Structural Chemistry, 2004, vol. 45, no. 5, pp. 838-843. Available at: https://link.springer.com/content/pdf/10.1007%2Fs10947-005-0066-x.pdf
27. White A., Jiang S. Journal of Physical Chemistry B, 2011, vol. 115, no. 4, pp. 660-667. DOI: 10.1021/jp1067654 Available at: http://pubs.acs.org/doi/abs/10.1021/jp1067654 (accessed 21.09.2017)
28. Korolev V. P. Journal of Structural Chemistry, 2013, vol. 54, no. 3, pp. 534-540. DOI: 10.1134/S0022476613030098
29. Erdey-Gruz T. Transport Phenomena in Aqueous Solutions. Budapest, Akademiai Kiado Publ., 1974.
30. Kravtsov V. I. Equilibrium and Kinetics of Electrode Reactions of Metal Complexes. Moscow: Chemistry Publ., 1985, 208 p. (in Russian)
