Progesterone definition in some medical products by method of liquid chromatography in micellar mobile phases
Keywords:
high-performance liquid chromatography, thin-layer chromatography, cationic, anionic and not ionic surfactants, progesterone.
Abstract
Chromatographic behavior of a female sexual hormone – a progesterone in micellar mobile
phases on the basis of cationic, anionic and not ionic surfactants by the methods of high-performance
liquid and thin-layer chromatography is studed. Techniques of quantitative definition of progesterone in
some medical products in micellar mobile phases on the basis dodecilsulfat sodium are developed
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References
1.Резников А. Г. Методы определения гормонов. К.: Наук. думка, 1980. 536с.
2.Герег Ш. Количественный анализ стероидов. М: Мир, 1985. 504с.
3.Kreuzer M.P., McCarthy R., Pravda M., Guilbault G.G. Development of
electrochemical immunosensor for progesterone analysis in milk // Anal. Lett. 2004. V.37,
№ 5. P. 943-956.
4.Srivastava M.L., Tiwari A.K., Mishra M.K. Electrophoresis of progesterone particles
dispersed in carbohydrate and nonelectrolyte solutions // J. Colloid and Interface Sci. 2002.
V.249, №2. P.322-326.
5.Shiwei Xu. Спектрофотометрическое определение 1,4-3-кетостероидов // Anal.
Chem. 1987. V.15, №5. P.385-389.
6.Гончаров Н.П., Кация Г.В., Колесникова Г.С., Нижник А.Н. и др. Сравнительный
анализ определения тестостерона в сыворотке крови различными методами // Журн.
пробл. эндокринологии. 2005. Т.51, №6. С.31-37.
7.Lovgren U., Kronkvist K., Johansson G., Edholm L.-E. Enzym amplified immunoassay
for steroids in biosamples at low picomolar concentrations // Anal. Chim. Acta. 1994.
V.288, №3. P.227-235.
8.Zherdev A.V., Byzova N.A., Izumrudov V.A. Rapid polyelectrolyte-based
immunofiltration technique for testosterone detection in serum samples // Analyst. 2003.
V.128, №10. P.1275-1280.
9.Jungju S., Hye-Young K., Chul C.B., Jungju Seo H.J. Simultaneous determination of
anabolic steroids and synthetic hormones in meat by freezing-lipid filtration, solid-phase
extraction and gas chromatography-mass spectrometry // J. Chromatogr. A. 2005. V.1067,
№1-2. P.303-309.
10. Marcos V., Perogordo E., Espinosa P., Martin de Pozuelo M., Hooghuis H.
Multiresidue analysis of anabolic compounds in bovine hair by gas chromatographytandem
mass spectrometry // Anal. chim. acta. 2004. V.507, №2. P. 219-227.
11. Adessi G.L., Eichenberger D., Quang Nhuan Tran, Jayle N.F. Gas chromatography
profile of estrogens: Application to pregnancy urine // Steroids. 1975. V.25, №4. P.553-
564.
12. Balizs G., Jainz A., Horvatovich P. Investigation of the feeding effect on the
13C/12C isotope ratio of the hormones in bovine urine using gas
chromatography/combustion isotope ratio mass spectrometry // J. Chromatogr. A. 2005.
V.1067, №1-2. P.323-330.
13. Tinschert K., Träger L. Separation of androsterone from epiandrosterone, and
dehydroepiandrosterone from its 3-hydroxy epimer by thin-layer chromatography // J.
Chromat. 1978. V.152, №2. P.447-452.
14. Lekic M., Korac F., Sober M., Marjanovic A. Planar chromatography of steroid
hormones and anabolics // Acta chim. sloven. 2007. V.54, №1. P.88-91.
15. Zarzycki P.K., Zarzycka M.B. Application of temperature-controlled micro planar
chromatography for separation and quantification of testosterone and its derivatives // J.
Anal. and Bioanal. Chemistry. 2008. V.391, №6. P.2219-2225.
16. Carfagnini G., Corcia A.Di, Marchetti M., Samperi R. Assay for urinary estriol
during the menstrual cycle based on extraction by a graphitized carbon black cartridge
followed by high-performance liquid chromatography // Chromatog. 1987. V.23, №11. P.
835-838.
17. Batra S.K., Saumande J. High Performance Liquid Chromatographic Separation of
Estradiol-17 and -17β in Biological Fluids; Application to Plasma, Milk and Urine of
Cows // J. Liquid Chromatogr. & Relat. Technol. 1984. V.7, №12. P.2431-2446.
18. Zhao Shan, Wu Danan, Wang Peng. Simultaneous determination of seven sexual
hormones in cosmetics by reversed-phase high performance liquid chromatography //
Chin. J. Chromatogr. 2004. V.22, №3. P.267-269.
19. Reddy S., Iden C.R., Brownawell B.J. Analysis of steroid conjugates in sewage
influent and effluent by liquid chromatography-tandem mass spectrometry // Anal. Chem.
2005. V.77, №21. P. 7032-7038.
20. Ingrand V., Herry G., Beausse J., de Roubin M. R. Analysis of steroid hormones in
effuents of wastewater treatment plants by liquid chromatoraphy-tandem mass
spectrometry // J. Chromatogr. A. 2003. V.1020, №1. P.95-100.
21. Koh Y.K.K., Chiu T.Y., Boobis A., Cartmell E., Lester J.N. and Scrimshaw M.D.
Determination of steroid estrogens in wastewater by high performance liquid
chromatography-tandem mass spectrometry // J. Chromatogr. A. 2007. V.1173, №1-2.
P.81-87.
22. Petrovic M., Tavazzi S., Barcelo D. Column-switching system with restricted access
pre-column packing for an integrated sample cleanup and liquid chromatographic-mass
spectrometric analysis of alkylphenolic compounds and steroid sex hormones in sediment
// J. Chromatogr. A. 2002. V.971, №1-2. P.37-45.
23. Карцова Л.А., Стрельникова Е.Г. Разделение экзо- и эндогенных стероидных
горомнов мицеллярной высокоэффективной тонкослойной хроматографией // Журн.
аналит. химии. 2007. Т.62, №9. С.965-968.
24. Garcia Diez L., H.-J. Bart Micellar chromatography for enantiomer separations // 27
International Exhibition-Congress on Chemical Engineering, Environmental Protection and
Biotechnology, Frankfurt am Main. 19-24 May, 2003. P.74.
25. Шатц В.Д., Сахартова О.В. Высокоэффективная жидкостная хроматография.
Рига, 1988. 160с.
26. Сумина Е.Г., Штыков С.Н., Тюрина Н.В. Поверхностно-активные вещества в
тонкослойной хроматографии. // Журн. аналит. химии. 2003. Т.58, №8. С.808-818.
2.Герег Ш. Количественный анализ стероидов. М: Мир, 1985. 504с.
3.Kreuzer M.P., McCarthy R., Pravda M., Guilbault G.G. Development of
electrochemical immunosensor for progesterone analysis in milk // Anal. Lett. 2004. V.37,
№ 5. P. 943-956.
4.Srivastava M.L., Tiwari A.K., Mishra M.K. Electrophoresis of progesterone particles
dispersed in carbohydrate and nonelectrolyte solutions // J. Colloid and Interface Sci. 2002.
V.249, №2. P.322-326.
5.Shiwei Xu. Спектрофотометрическое определение 1,4-3-кетостероидов // Anal.
Chem. 1987. V.15, №5. P.385-389.
6.Гончаров Н.П., Кация Г.В., Колесникова Г.С., Нижник А.Н. и др. Сравнительный
анализ определения тестостерона в сыворотке крови различными методами // Журн.
пробл. эндокринологии. 2005. Т.51, №6. С.31-37.
7.Lovgren U., Kronkvist K., Johansson G., Edholm L.-E. Enzym amplified immunoassay
for steroids in biosamples at low picomolar concentrations // Anal. Chim. Acta. 1994.
V.288, №3. P.227-235.
8.Zherdev A.V., Byzova N.A., Izumrudov V.A. Rapid polyelectrolyte-based
immunofiltration technique for testosterone detection in serum samples // Analyst. 2003.
V.128, №10. P.1275-1280.
9.Jungju S., Hye-Young K., Chul C.B., Jungju Seo H.J. Simultaneous determination of
anabolic steroids and synthetic hormones in meat by freezing-lipid filtration, solid-phase
extraction and gas chromatography-mass spectrometry // J. Chromatogr. A. 2005. V.1067,
№1-2. P.303-309.
10. Marcos V., Perogordo E., Espinosa P., Martin de Pozuelo M., Hooghuis H.
Multiresidue analysis of anabolic compounds in bovine hair by gas chromatographytandem
mass spectrometry // Anal. chim. acta. 2004. V.507, №2. P. 219-227.
11. Adessi G.L., Eichenberger D., Quang Nhuan Tran, Jayle N.F. Gas chromatography
profile of estrogens: Application to pregnancy urine // Steroids. 1975. V.25, №4. P.553-
564.
12. Balizs G., Jainz A., Horvatovich P. Investigation of the feeding effect on the
13C/12C isotope ratio of the hormones in bovine urine using gas
chromatography/combustion isotope ratio mass spectrometry // J. Chromatogr. A. 2005.
V.1067, №1-2. P.323-330.
13. Tinschert K., Träger L. Separation of androsterone from epiandrosterone, and
dehydroepiandrosterone from its 3-hydroxy epimer by thin-layer chromatography // J.
Chromat. 1978. V.152, №2. P.447-452.
14. Lekic M., Korac F., Sober M., Marjanovic A. Planar chromatography of steroid
hormones and anabolics // Acta chim. sloven. 2007. V.54, №1. P.88-91.
15. Zarzycki P.K., Zarzycka M.B. Application of temperature-controlled micro planar
chromatography for separation and quantification of testosterone and its derivatives // J.
Anal. and Bioanal. Chemistry. 2008. V.391, №6. P.2219-2225.
16. Carfagnini G., Corcia A.Di, Marchetti M., Samperi R. Assay for urinary estriol
during the menstrual cycle based on extraction by a graphitized carbon black cartridge
followed by high-performance liquid chromatography // Chromatog. 1987. V.23, №11. P.
835-838.
17. Batra S.K., Saumande J. High Performance Liquid Chromatographic Separation of
Estradiol-17 and -17β in Biological Fluids; Application to Plasma, Milk and Urine of
Cows // J. Liquid Chromatogr. & Relat. Technol. 1984. V.7, №12. P.2431-2446.
18. Zhao Shan, Wu Danan, Wang Peng. Simultaneous determination of seven sexual
hormones in cosmetics by reversed-phase high performance liquid chromatography //
Chin. J. Chromatogr. 2004. V.22, №3. P.267-269.
19. Reddy S., Iden C.R., Brownawell B.J. Analysis of steroid conjugates in sewage
influent and effluent by liquid chromatography-tandem mass spectrometry // Anal. Chem.
2005. V.77, №21. P. 7032-7038.
20. Ingrand V., Herry G., Beausse J., de Roubin M. R. Analysis of steroid hormones in
effuents of wastewater treatment plants by liquid chromatoraphy-tandem mass
spectrometry // J. Chromatogr. A. 2003. V.1020, №1. P.95-100.
21. Koh Y.K.K., Chiu T.Y., Boobis A., Cartmell E., Lester J.N. and Scrimshaw M.D.
Determination of steroid estrogens in wastewater by high performance liquid
chromatography-tandem mass spectrometry // J. Chromatogr. A. 2007. V.1173, №1-2.
P.81-87.
22. Petrovic M., Tavazzi S., Barcelo D. Column-switching system with restricted access
pre-column packing for an integrated sample cleanup and liquid chromatographic-mass
spectrometric analysis of alkylphenolic compounds and steroid sex hormones in sediment
// J. Chromatogr. A. 2002. V.971, №1-2. P.37-45.
23. Карцова Л.А., Стрельникова Е.Г. Разделение экзо- и эндогенных стероидных
горомнов мицеллярной высокоэффективной тонкослойной хроматографией // Журн.
аналит. химии. 2007. Т.62, №9. С.965-968.
24. Garcia Diez L., H.-J. Bart Micellar chromatography for enantiomer separations // 27
International Exhibition-Congress on Chemical Engineering, Environmental Protection and
Biotechnology, Frankfurt am Main. 19-24 May, 2003. P.74.
25. Шатц В.Д., Сахартова О.В. Высокоэффективная жидкостная хроматография.
Рига, 1988. 160с.
26. Сумина Е.Г., Штыков С.Н., Тюрина Н.В. Поверхностно-активные вещества в
тонкослойной хроматографии. // Журн. аналит. химии. 2003. Т.58, №8. С.808-818.
Published
2019-11-26
How to Cite
Sumina, E. G., Sorokina, O. N., Uglanova, V. Z., & Belaya, E. V. (2019). Progesterone definition in some medical products by method of liquid chromatography in micellar mobile phases. Sorbtsionnye I Khromatograficheskie Protsessy, 11(5). Retrieved from https://journals.vsu.ru/sorpchrom/article/view/1974
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