Gas mixtures of the known composition by dynamic methods
Keywords:
calibration gas mixtures, gas chromatography, static methods, dynamic methods, polybubbler method, chromato-desorbtion method.
Abstract
In the paper modern methods of obtaining gas mixtures of known composition are considered. This
gas mixtures characterized by stable for a time sufficient for the calibration carrying out. The features of dynamic
methods that have received the greatest practical application over a period of 15-20 years in Russian
and foreign source are discussed. The results of comparative analysis of the accuracy of preparation of gas
mixtures of volatile organic compounds by diffusion, polybubbler and chromato-desorption methods are presented.
The results of a comparison of the accuracy of preparation of gas mixtures of volatile organic compounds
by diffusion, polybubbler and chromato-desorption methods are presented. It is shown that the application
of chromato-desorption devices allows to obtain gas mixtures that stable for 10-60 hours in a dynamic
condition. This gas mixtures contain volatile aliphatic and aromatic hydrocarbons with an error no more than
7%. The chromato-desorption method is equal to the polybubbler and diffusion methods of obtaining gas
mixtures, but there is decreasing of the consumption of reagents by a decade.
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References
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2. Brewer P.J., Brown R.J.C., Miller M.N., Minarro M.D. et al., Analytical Chemistry , 2014, Vol. 86, No 3, pp. 1887-1893.
3. Słomińska M., Konieczka P., Namieśnik J., Trends in Analytical Chemistry, 2014, No 62, pp. 135-143.
4. Armenta S., Garrigues S., de la Guardia M., Trends in Analytical Chemistry, 2008, Vol. 27, No 6, pp. 497-511.
5. Grenfell R.J.P., Milton M.J.T., Harling A.M., Vargha G.M. et al., Journal of Geophysical Research Atmospheres, 2010, Vol. 115, No 14, pp. 1-4.
6. Kuklinska K., Wolska L., Namiesnik J., Atmospheric Pollution Research, 2015, Vol.6, No 1, pp. 129-137.
7. Tsai. C.J., Aggarwal S.G., Mapan – Jornal of Metrology Society of India, 2013, Vol. 28, No 3, pp. 141-143.
8. Kustikov Y.A., Popov B.I., Mapan -Journal of Metrology Society of India, 2013, Vol. 28, No 3, pp. 181-191.
9. McKinley J., Majors R.E., Reprinted from LCGC, 2000, Vol. 18, No 10, pp. 1-6.
10. Gas analysis - Preparation of calibration gas mixtures using dynamic volumetric methods - Parts 1-10 // International standard. Geneva. ISO 6145.
11. Milton M. J.T., Vargha G.M., Brown A.S., Metrologia, 2011, Vol. 48, No 5, pp. 1-9.
12. Nishino T., Harusue T., Maruyama M., Bunseki Kagaku, 2006, Vol. 55, No 3, pp. 199-203.
13. Matsumoto N., Shimosaka T., Watanabe T., Kato K., Analytical and Bioanalytical Chemistry, 2008, Vol. 391, No 6, pp. 2061-2069.
14. Watson J.G., Chow J.C., Tropp R.J., Kohl S.D. et al., Mapan - Journal of Metrology Society of India, 2013, Vol. 28, No 3, pp. 167-179.
15. Knopf D., Accreditation and Quality Assurance, 2011, Vol. 6, No 3, pp. 113-119.
16. Rhoderick G.C., Analytical and Bioanalytical Chemistry, 2013. Vol. 405, No 1, pp. 369-375.
17. Gerboles M., Diaz E., Noriega-Guerra A.,/Accreditation and Quality Assurance, 1998, Vol. 3, No 2, pp. 69-78.
19. Matsumoto, N., Takada K., Shimosaka T., Accreditation and Quality Assurance, 2016, Vol. 21, No 5, pp. 335-339.
20. Xiang J., Mo J., Wan H., Zhang Y., Li M., Indoor Air 2014 – 13th International Conference on Indoor Air Quality and Climate, 2014, pp. 200-205.
21. Hu S., Wu H., Wang D., Li J., Measurement: Journal of the International Measurement Confederation, 2013, Vol. 46 (3), pp. 1084-1088.
23. Richter M., Jann O., Horn W., Pyza L. et al., Gefahrstoffe Reinhaltung der Luft, 2013, Vol. 73 (3), pp. 103-106.
24. Brewer P.J., Miñarro M.D., Di Meane E.A., Brown R.J.C., Measurement: Journal of the International Measurement Confederation, 2014, Vol. 47 (1), pp. 607-612.
25. Budovich V.L., Polotnyuk E.B., Inorganic Materials., 2009, Vol. 45, No 14, pp. 1555-1558.
26. Świtaj-Zawadka A., Konieczka P., Szczygelska-Tao J., Biernat J.F. et al, Journal of Chromatography A, 2004, Vol. 145-151.
27. Thorenz U.R., Kundel M., Müller L., Hoffmann T., Analytical and bioanalytical Chemistry, 2012, Vol. 404, No 8, pp. 2177-2183.
28. Choi M.F., Hawkins P., Analytical Chemistry, 1997, Vol. 69, No 6, pp. 1237-1239.
29. Tumbiolo S., Vincent L., Gal J.-F., Maria P.-C., Analyst, 2005, Vol. 130, No 10, pp.1369-1374.
30. Zhou Z., Gai L., Accreditation and Quality Assurance, 2006, Vol. 11 (4), pp. 205-207.
31. Tompson J.M., Perry D.B., Journal of Environmental Monitoring, 2009, Vol. 11 (8), pp. 1543-1544.
32. Abe H, Kitano H., Matsumoto N., Takahashi C., Metrologia, 2015, Vol. 52 (6), pp. 731-740.
33. Susaya J., Kim K.-H., Cho J., Parker D., Journal of Chromatography A, 2012, No 1225, pp. 8-16.
34. Jardine K. J., Henderson W. M., Huxman T.E., Abrell L., Atmos. Meas. Tech,. 2010, No 3, pp. 1569-1576.
35. Rodinkov O.V., Moskvin L.N., Rathour J.K.. Journal of Analytical Chemistry, 2004, Vol. 59(11), pp. 1073-1078.
36. Rodinkov O.V., Moskvin L.N., Vas'kova E.A., Russian Journal of Physical Chemistry A, 2005, Vol. 79(3), pp. 453-456.
37. Rodinkov O.V., Rachkovskii I.N., Moskvin L.N., Journal of Analytical Chemistry, 2008, Vol. 63(9), pp. 857-862.
38. Moskvin L.N., Rodinkov O.V., Russian Chemical Bulletin, 2012, Vol. 61(4), pp. 723-740.
39. Rodinkov O.V., Moskvin L.N., Viktorova M.I., Dyakin A.A. et al., Chromatographia, 2015, Vol. 78(17-18), pp. 1211-1220.
40. Moskvin L.N., Rodinkov O.V., Theoretical Foundations of Chemical Engineering, 2016, Vol. 50(4), pp. 655-659.
41. Naganowska-Nowak A., Koniczka P., Przyjazny A., Namieśnik J., Critical Reviews in Analytical Chemistry, 2005, Vol. 35 (1), pp. 31-55.
42. Słomińska M., Konieczka P., Namieśnik J., TrAC – Trends in Analytical Chemistry, 2014, Vol. 62, pp. 135-143.
43. Przyk E., Konieczka P., Szczygelska-Tao J., Biernat J.F., et al., Journal of Separation Science, 2001, Vol. 24 (3), pp. 226-229.
44. Konieczka P., Prokopowicz M., Zygmunt B., Biernat J.F., Namieśnik J., Chromatographia, 2000, Vol. 51(2), pp. S249-S260.
45. Mofidi A., Asilian H. , Jafari A.J., Iran Occupational Healt, 2014, Vol. 11, No 2, pp. 75-87.
46. Li Y., Täffner T., Bischoff M., Niemeyer B., International Journal of Chemical Engineering, 2012, Article number 417029.
47. Vitenberg A.G., Konopel'ko L.A., Journal of Analytical Chemistry, 2011, Vol. 66(5), pp.438-457.
48. Vitenberg A.G., Dobryakov Yu.G., Gromysh E.M., Journal of Analytical Chemistry, 2010, 65(12), pp. 1284-1290.
49. Vitenberg A.G , Journal of Analytical Chemistry, 2003, Vol.58(1), pp. 2-15.
50. Vitenberg A.G. Journal of Analytical Chemistry, 2003, Vol. 8(1), pp. 1-2.
51. Platonov I.A., Ismagilov D.R., Kudryashov S.Yu., Smygina I.N. et al., Journal of Analytical Chemistry, 2006, Vol .61(1), pp. 52-57.
52. Berezkin V.G., Platonov I.A., Lepskii M.V., Ismagilov D.R. et al, Russian Journal of Physical Chemistry A, 2003, Vol. 77(7), pp. 1204-1206.
53. Platonov I.A., Arutunov Y.I.., Ismagilov D.R., Smygina I.N., Sorbtsionnye i khromatograficheskie protsessy, 2006, Vol. 6, No 4, pp. 581-590.
54. Platonov I.A., Sorbtsionnye i khromatograficheskie protsessy, 2006, Vol. 6.,No 5, pp. 833-843.
55. Berezkin V.G.., Platonov I.A., Smygina I.N., Izvestiya Vysshikh Uchebnykh Zavedeniy. Chemistry and chemical technology, 2007, Vol. 50, No 8, pp. 22-24.
56. Platonov I.A., Kolesnichenko I.N., Lange P.К., Metrologia, 2016, No 4, pp. 29-36.
57. Platonov I.A., Kolesnichenko I.N., Lobanova M.S., Micheenkova A.E., Рroceedings of the 12th international students conference modern analytical сhemistry, Prague. Czech republic. Sep. 22-23, 2016, pp.37-41.
58. Platonov I.A., Kolesnichenko I.N., Lobanova M.S., Micheenkova A.E., Рroceedings of the 12th international students conference modern analytical сhemistry, Prague. Czech republic. Sep. 22-23, 2016, pp. 42-48.
Published
2018-02-21
How to Cite
Колесниченко, И. Н., Платонов, И. А., Новикова, Е. А., & Муханова, И. М. (2018). Gas mixtures of the known composition by dynamic methods. Sorbtsionnye I Khromatograficheskie Protsessy, 17(3), 378-387. https://doi.org/10.17308/sorpchrom.2017.17/391
Section
Статьи
