Gas mixtures of the known composition by dynamic methods

  • И. Н. Колесниченко Kolesnichenko Irina N. - Ph.D. (chemistry), associate prof., department of chemistry, Samara National Research University, Samara
  • И. А. Платонов Platonov Igor A. - prof., grand Ph.D (chemistry), Head of chemistry department, Samara National Research University, Samara
  • Е. А. Новикова Novikova Ekaterina A. - Ph.D. (chemistry), associate prof., department of chemistry, Samara National Research University, Samara
  • И. М. Муханова Mukhanova Irina M. - Ph.D. (chemistry), associate prof., department of chemistry, Samara National Research University, Samara
Keywords: calibration gas mixtures, gas chromatography, static methods, dynamic methods, polybubbler method, chromato-desorbtion method.

Abstract

In the paper modern methods of obtaining gas mixtures of known composition are considered. This
gas mixtures characterized by stable for a time sufficient for the calibration carrying out. The features of dynamic
methods that have received the greatest practical application over a period of 15-20 years in Russian
and foreign source are discussed. The results of comparative analysis of the accuracy of preparation of gas
mixtures of volatile organic compounds by diffusion, polybubbler and chromato-desorption methods are presented.
The results of a comparison of the accuracy of preparation of gas mixtures of volatile organic compounds
by diffusion, polybubbler and chromato-desorption methods are presented. It is shown that the application
of chromato-desorption devices allows to obtain gas mixtures that stable for 10-60 hours in a dynamic
condition. This gas mixtures contain volatile aliphatic and aromatic hydrocarbons with an error no more than
7%. The chromato-desorption method is equal to the polybubbler and diffusion methods of obtaining gas
mixtures, but there is decreasing of the consumption of reagents by a decade.

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Published
2018-02-21
How to Cite
Колесниченко, И. Н., Платонов, И. А., Новикова, Е. А., & Муханова, И. М. (2018). Gas mixtures of the known composition by dynamic methods. Sorbtsionnye I Khromatograficheskie Protsessy, 17(3), 378-387. https://doi.org/10.17308/sorpchrom.2017.17/391