Preparation of standard gas and liquid media by chromato-desorption method
Abstract
The paper presents an analysis of modern techniques for producing gas and liquid media with a given concentration of analytes by the chromato-desorption method. The possibilities of dynamic and discrete static methods, approaches to miniaturization and automation of the process are shown. Using the example of fatty acids (FA), the possibilities of using monolithic chromate desorption systems (MHDS) to produce standard liquid media are presented. The paper compares the degree of LC extraction from MHDS based on various polymer materials in the static extraction mode at temperatures of 25, 50 and 80°C and a pressure of 17-18 MPa. It is shown that the extraction of LC from MHDS based on polyester resin with an error of maintaining constant concentrations not exceeding 10% is achieved with 5-6 immersion in the extraction medium. Ranges of detectable concentrations of LC in n-octane extracts obtained as a result of MHDS studies in the static extraction mode have been established: 3-17 g/m3, 6-36 g/m3, 8-66 g/m3 for tetradecanoic acid, 3-29 g/m3, 6-58 g/m3, 10-90 g/m3 for Pentadecanoic acid, 4-32 g/m3, 8-69 g/m3, 12-99 g/m3 for hexadecanoic acid, 4-42 g/m3, 10-89 g/m3, 15-143 g/m3 for octadecanoic acid. A comparison of the results of the analysis of solutions obtained as a result of MHDS studies based on various polymer materials in a static mode allows us to conclude that using MHDS based on polyester resin makes it possible to obtain highly concentrated LC solutions in nonpolar solvents. It is important to note that in order for the MHDS based on polyester resin to reach the quasi-stationary operating mode, it is necessary to spend more time compared with the samples of MHDS based on epoxy resin, where the output to the plateau of quasi-stationary concentrations was observed from 2, rather than from 5-6 immersion. For MHDS of a similar configuration, the stable operation time is noticeably reduced due to its weak resistance to nonpolar organic solvent and intensive extraction of LC.
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