Process control synthesis of imidazolines of saturated fatty acids by TLC and GC/MS methods
Keywords:
thin layer chromatography, gas chromatography-mass spectrometry, imidazolines, saturated fatty acids
Abstract
The chromatographic procedures for control of imidazolines synthesis based on interaction of
saturated fatty acids on an example of caprylic, capric and myristic with aminoethylethanolamine have been
represented. The optimal conditions of the thin layer chromatography for the determination of the conversion
of fatty acids are proposed. The structure of obtained imidazolines has been determined by gas
chromatography-mass spectrometry.
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application 20.12.78, patented 15.07.80.
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khromatografii (planarnaja khromatografija)
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Tonkosloinaja khromatografija v organicheskoy
himii. M.: Himija. 1978. 128 p.
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A.V. et al., Sorbtsionnye i khromatograficheskie
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33, No 4, pp. 343-353.
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78, No 9, pp. 881-888.
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and mass spectrometry: a practical guide. 2010.
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A.A. et al., Sorbtsionnye i khromatograficheskie
protsessy, 2014, Vol. 14, No 3, pp. 494-501.
11. GOST 23239 Kisloty zhirnye
sinteticheskie fraktciy S5-S6, S7-S9, S5-S9,
S10-S13, S10-S16, S17-S20. Tekhnicheskie
uslovija.
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of Wood Science, 2003, Vol. 49, No 4, pp. 371-
376.
Published
2018-02-19
How to Cite
Кружилин, А. А., Перегудова, А. С., Перелыгина, И. Э., Столповская, Н. В., & Фалалеев, А. В. (2018). Process control synthesis of imidazolines of saturated fatty acids by TLC and GC/MS methods. Sorbtsionnye I Khromatograficheskie Protsessy, 15(3), 464-472. https://doi.org/10.17308/sorpchrom.2015.15/295
Section
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