Planar complexation chromatography of transition metal ions
Keywords:
: thin layer chromatography, modified silica gels, chelate agents, iminodiacetic acid, transition metals
Abstract
The method for analysis of transition metal ions (Zn(II), Cu(II), Со(II), Ni(II), Fe(III)) by high-performance planar (thin layer) chromatography with the use of sorbents modified by chelating fragments of iminodiacetic acid was developed. The correlation between retention factor (Rf) and physico-chemical parameters of the separated systems was studied. It was demonstrated that unlike the pH value, ionic strength of a solution does not exert significant influence on resolution and mobility of transition metal cations
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References
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2. Pupishev A.A., Atomno-absorbtsionnii spektralnii analyz. М., Tehnosphera, 2009, 784 p.
3. ZolotovYu. А., Ivanov V. М., AmelinV.G., Himicheskie test-меtodi analiza. M.: Editirial URSS, 2002. 304 p.
4. Fritz J.S., Gjerde D.T. Ion Chromatography, Wiley-VCH Verlag, Weinheim, 2009, 385 p.
5. Volinets М.P., Kolichstvennaya tonkosloinaya hromatographiya v neorganichskom analyze . М., Nauka, 1993. 240 p.
6. Malakhova I.I., Belyaev А.N., Krasikov V.D., Sorbtsionnye i khromatograficheskie protsessy, 2015, Vol. 15, No 6, pp. 802-810.
7. Nesterenko P.N., Djons F., Poll B., М. Tehnosphera, 2013, 312 p..
8. Herring R., Helatoobrazuyschie ionoobmenniki,. М., Мir, 1971, 280 p.
9. Myasoedova G.B., Savvin S.B., Helatoobrazuyschie sorbenti, М., Himiya, 1984, 171 p.
10. Jones P., Challenger O.J., Hill S.J. Recent advances in high-performance chelation ion chromatography for trace-metal determinations, in Ion Exchange Processes: Advances and Applications, ed. A. Dyer, M.J. Hudson, P.A. Williams, Royal Society of Chemistry, Cambridge, 1993, pp.279-287.
11. Frits Dj., GierdeD., Poland К. Ionnayahromatographya, М., Мir, 1984, 221 p.
12. Bonn G.K., Nathakarnkitkool S., Jandik P., Coordination chromatography of transition metals: efficient and selective separations of cations on iminodiacetate functional groups, in Advances in Ion Chromatography, ed. P. Jandik and R.M. Cassidy, Century International, Medfield, MA, 1991, pp. 197-214.
13. Jones P., Nesterenko P.N., Chelation ion chromatography, in Encyclopedia of Analytical Science, ed. P.J. Worsfold, A. Townsend and C.E. Poole, Academic Press, Amsterdam, 2004, pp. 467-480.
14. Tria J., Haddad P.R., Nesterenko P.N., J. Separation Science, 2008, Vol. 31, pp. 2231-2238.
15. Bashir W., Paull B., J. Chromatogr A, 2001, Vol. 907, pp. 191-200.
16. Nesterenko P.N., Jones P., J. Chromatogr. A, 1988, Vol. 804, pp. 223-231.
17. Ailer R.К. Himiya kremnezema. М., Мir. 1982, Vol. 1,2. 712 p.
18. Busche B., Wiacek R., Davidson J., Koonsiripaiboon V. et al., Chem. Commun. 2009, Vol. 12, pp. 312-315
Published
2018-02-22
How to Cite
Малахова, И. И., Красиков, В. Д., Горшков, Н. И., Беляев, А. Н., & Староверов, С. М. (2018). Planar complexation chromatography of transition metal ions. Sorbtsionnye I Khromatograficheskie Protsessy, 17(4), 682-688. https://doi.org/10.17308/sorpchrom.2017.17/428
Section
Статьи
