Sorptive resolution of phenolic acids in ion-pair reversed-phase HPLC
Keywords:
HPLC, retention, phenolic acids, ion-pair chromatography.
Abstract
In the paper it has been shown that exploration of the ion-pair mode (by addition of
cetyltriethylammonim nitrate) of reversed-phase HPLC with Kromasil-100 5C18 stationary phase permits
to change to an opposite sequence of phenolic acids (caffeic, p-cumaric, ferulic and sinapic) elution. The
particularities of the ion-pair mode are discussed
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References
1. Stalikas C.D. Phenolic Acids and Flavonoids: Occurrence and Analytical Methods / In
«Free Radicals and Antioxidant Protocols» (Methods in Molecular Biology 610). Ed. R.M.
Uppu et al. Humana Press, a part of Springer Science+Business Media, LLC. 1998, 2010.
- Chapter 5. – P. 65-90.
2. Fleuriet A., Macheix J.-J. Phenolic acids in fruits and vegetables / In «Flavonoids in
health and disease». Second edition. Revised and expanded. Ed. Catherine Rice-
Evans,Lester Packer. Marcel Deckker, Ink., New York. – 2003. – P. 1-42.
3. Hollman P.C.H. Evidence for health benefits of plant phenols: local or systemic
effects? // J. Sci. Food Agric. – 2001. – V.81. – P. 842-852.
4. Kawamura K.; Okuwaki A., Verheyen T.V., Perry G.J. Separation of Aromatic
Carboxylic Acids Using Quaternary Ammonium Salts on Reversed-Phase HPLC. 1.
Separation Behavior of Aromatic Carboxylic Acids // Separation Science and Technology,
Volume 41, Issue 2 February 2006 , pages 379 - 390
5. Дейнека В.И. Карта хроматографического разделения и инкрементные
зависимости в методе относительного анализа удерживания в ВЭЖХ // Ж. физ.
химии. - 2006. - T.80. - С. 511-516.
6. Katritzky A.R., Karelson M., Lobanov V.S. QSPR as a means of predicting and
understanding chemical and physical properties in terms of structure // Pure Appl. Chem. –
1997. - V.69. – P. 245-248.
7. Дейнека В.И. Метод анализа относительного удерживания в ВЭЖХ.
Определение, применения и роль параметра lgP системы н-октанол – вода. Ж. физ.
химии. - 2006. - T.80. - С. 1083-1088.
8. Cecchi T. «Ion-pair chromatography and related techniques» (Analytical chemistry
series). CRS Press Taylor and Francis. 2010. – P. 29-39.
9. Katz S., Pitt W.W., Jr., Johnes G., Jr. Sensitive fluorescence monitoring of aromatic
acids after anion-exchange chromatogramphy of body fluids // Clin. Chem. – 1973. – V.19.
- P. 817-820.
«Free Radicals and Antioxidant Protocols» (Methods in Molecular Biology 610). Ed. R.M.
Uppu et al. Humana Press, a part of Springer Science+Business Media, LLC. 1998, 2010.
- Chapter 5. – P. 65-90.
2. Fleuriet A., Macheix J.-J. Phenolic acids in fruits and vegetables / In «Flavonoids in
health and disease». Second edition. Revised and expanded. Ed. Catherine Rice-
Evans,Lester Packer. Marcel Deckker, Ink., New York. – 2003. – P. 1-42.
3. Hollman P.C.H. Evidence for health benefits of plant phenols: local or systemic
effects? // J. Sci. Food Agric. – 2001. – V.81. – P. 842-852.
4. Kawamura K.; Okuwaki A., Verheyen T.V., Perry G.J. Separation of Aromatic
Carboxylic Acids Using Quaternary Ammonium Salts on Reversed-Phase HPLC. 1.
Separation Behavior of Aromatic Carboxylic Acids // Separation Science and Technology,
Volume 41, Issue 2 February 2006 , pages 379 - 390
5. Дейнека В.И. Карта хроматографического разделения и инкрементные
зависимости в методе относительного анализа удерживания в ВЭЖХ // Ж. физ.
химии. - 2006. - T.80. - С. 511-516.
6. Katritzky A.R., Karelson M., Lobanov V.S. QSPR as a means of predicting and
understanding chemical and physical properties in terms of structure // Pure Appl. Chem. –
1997. - V.69. – P. 245-248.
7. Дейнека В.И. Метод анализа относительного удерживания в ВЭЖХ.
Определение, применения и роль параметра lgP системы н-октанол – вода. Ж. физ.
химии. - 2006. - T.80. - С. 1083-1088.
8. Cecchi T. «Ion-pair chromatography and related techniques» (Analytical chemistry
series). CRS Press Taylor and Francis. 2010. – P. 29-39.
9. Katz S., Pitt W.W., Jr., Johnes G., Jr. Sensitive fluorescence monitoring of aromatic
acids after anion-exchange chromatogramphy of body fluids // Clin. Chem. – 1973. – V.19.
- P. 817-820.
Published
2019-11-27
How to Cite
Anisimovich, I. P., Deineka, V. I., Deineka, L. A., Simakov, S. V., & Selemenev, V. F. (2019). Sorptive resolution of phenolic acids in ion-pair reversed-phase HPLC. Sorbtsionnye I Khromatograficheskie Protsessy, 10(4). Retrieved from https://journals.vsu.ru/sorpchrom/article/view/2078
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