Comprehensive quality control of butter using GRF, DSC and chemical analysis

  • Igor A. Saranov Voronezh State University of Engineering Technologies, Voronezh, Russian Federation
  • Vladimir F. Selemenev Voronezh State University, Voronezh, Russian Federation
  • Oleg B. Rudakov Voronezh State Technical University, Voronezh, Russian Federation
  • Alexander V. Vostroilov 4Voronezh State Agrarian University named after Emperor Peter I, Voronezh, Russian Federation
  • Konstantin K. Polyansky Voronezh Branch of the Russian University of Economics, Plekhanova G.V, Voronezh, Russian Federation
Keywords: cow's milk fat, storage capacity, oxidative damage, gas-liquid chromatography, differential scanning calo-rimetry, peroxide number, anisidine number, acid number.

Abstract

The composition of fatty acids (FA), triacylglycerols (TAG), and differential scanning calorimetry (DSC) were studied by the GC method, the thermophysical properties of butter were determined, and the relationship between the results obtained by these methods was traced. The dynamics of the oxidation of butter by atmospheric oxygen at room temperature has been studied using a set of certified chromatographic techniques, an alternative technique based on the DSC method, as well as chemical methods for determining integral oxidation indices (determination of peroxide, anisidine and acid numbers). The objects of the study were samples of butter produced from the milk of cows of Holstein, Montbilliard and Jersey breeds, which are bred in the south of the Voronezh region. It was found that the composition of LC and TAG for 18 days of storage at room temperature remains within the normalized ranges, at the same time, the formation of oxidation products is recorded by all methods used. The relatively better storage capacity of butter from milk of the Holstein breed has been established in comparison with butter from milk of cows of the Montbilliard and Jersey breeds.

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Author Biographies

Igor A. Saranov, Voronezh State University of Engineering Technologies, Voronezh, Russian Federation

Candidate of Technical Sciences, Associate Professor of the Department of Information Security of the Voronezh State University of Engineering Technologies, Voronezh, Russian Federartoin

Vladimir F. Selemenev, Voronezh State University, Voronezh, Russian Federation

Doctor of Chemical Sciences, Professor of the Department of Analytical Chemistry of Voronezh State University, Voronezh, Russian Federation

Oleg B. Rudakov, Voronezh State Technical University, Voronezh, Russian Federation

Doctor of Chemical Sciences, Head of Department of Chemistry and Chemical Technology of Materials of Voronezh State Technical University, Voronezh, Russian Federation

Alexander V. Vostroilov, 4Voronezh State Agrarian University named after Emperor Peter I, Voronezh, Russian Federation

Doctor of Agricultural Sciences, Head of the Department of Private Zootechny of Voronezh State Agrarian University, Voronezh, Russian Federation

Konstantin K. Polyansky, Voronezh Branch of the Russian University of Economics, Plekhanova G.V, Voronezh, Russian Federation

Doctor of Technical Sciences, Professor of the Department of Management of Socio-Economic Systems and Business Processes of the Voronezh Branch of Plekhanov Russian University of Economics, Voronezh, Russian Federation

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Published
2025-06-13
How to Cite
Saranov, I. A., Selemenev, V. F., Rudakov, O. B., Vostroilov, A. V., & Polyansky, K. K. (2025). Comprehensive quality control of butter using GRF, DSC and chemical analysis. Sorbtsionnye I Khromatograficheskie Protsessy, 25(2), 160-170. https://doi.org/10.17308/sorpchrom.2025.25/12955

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